| N1-C1 | 1.336(6) | C13-N2-C14 | 113.8(3) |
| N1-C5 | 1.338(6) | C7-O1-C6 | 121.2(4) |
| O8-C30 | 1.227(6) | N2-C13-N3 | 107.1(4) |
| Complex 2 [Cu(hfac)2(NIT-3PyPh)2] | |||
| Bond | Length(Å) | Bond | Angle(˚) |
| Cu1-O4 | 1.9733(14) | O4-Cu1-N1# | 89.71(6) |
| Cu1-N1 | 2.0589(17) | O4-Cu1-N1 | 90.30(6) |
| Cu1-O5 | 2.2802(15) | O4#-Cu1-N1 | 90.29(6) |
| N1-C3 | 1.344(3) | O4#-Cu1-N1# | 89.70(6) |
| N1-C2 | 1.346(3) | N1-Cu1-N1# | 180.00(9) |
| N3-O2 | 1.273(2) | O4-Cu1-O5 | 87.17(6) |
| N3-C13 | 1.353(3) | N1-Cu1-O5# | 87.96(6) |
| N3-C15 | 1.495(3) | N1-Cu1-O5 | 92.04(6) |
| O3-C7 | 1.363(3) | O5-Cu1-O5# | 180.00(7) |
| O3-C6 | 1.432(3) | C3-N1-C2 | 117.09(2) |
| O1-N2 | 1.278(2) | O2-N3-C13 | 126.9(2) |
| N2-C13 | 1.356(3) | O2-N3-C15 | 121.36(2) |
| N2-C14 | 1.504(3) | C13-N3-C15 | 111.67(2) |
| C22-O5 | 1.233(2) | C7-O3-C6 | 118.47(2) |