| Complex 1 {[Cu(hfac)2]2(NIT-4PyPh)}2 | |||
| Bond | Length(Å) | Bond | Angle(˚) |
| Cu1-O7 | 1.931(3) | O7-Cu1-O4 | 164.41(1) |
| Cu1-O4 | 1.933(3) | O7-Cu1-O2 | 93.04(1) |
| Cu1-O2 | 1.941(3) | O4-Cu1-O2 | 83.31(1) |
| Cu1-O5 | 1.978(3) | O7-Cu1-O5 | 89.96(1) |
| Cu1-O6 | 2.200(3) | O4-Cu1-O5 | 91.86(1) |
| Cu2-O9 | 1.939(3) | O2-Cu1-O5 | 172.09(1) |
| Cu2-O3 | 2.588(4) | O7-Cu1-O6 | 90.31(1) |
| Cu2-O11 | 1.948(3) | O4-Cu1-O6 | 105.19(1) |
| Cu2-O10 | 1.970(3) | O2-Cu1-O6 | 98.18(1) |
| Cu2-N1 | 1.999(4) | O5-Cu1-O6 | 89.12(1) |
| Cu2-O8 | 2.210(3) | O3-Cu2-O8 | 175.21(4) |
| O7-C27 | 1.277(5) | O9-Cu2-O11 | 175.15(2) |
| O5-C22 | 1.252(6) | O9-Cu2-O10 | 87.99(2) |
| O2-N2 | 1.302(4) | O11-Cu2-O10 | 90.77(2) |
| O4-C20 | 1.242(5) | O9-Cu2-N1 | 92.55(2) |
| N3-O3 | 1.263(5) | O11-Cu2-N1 | 87.85(2) |
| N3-C13 | 1.356(5) | O10-Cu2-N1 | 170.00(2) |
| N3-C15 | 1.501(5) | O9-Cu2-O8 | 90.72(1) |
| O6-C25 | 1.230(5) | O11-Cu2-O8 | 94.04(1) |
| N2-C13 | 1.333(5) | O10-Cu2-O8 | 94.17(1) |
| N2-C14 | 1.492(6) | N1-Cu2-O8 | 95.80(2) |
| O11-C37 | 1.241(6) | N3-O3-Cu2 | 161.69(3) |
| O9-C32 | 1.267(6) | N2-O2-Cu1 | 119.45(8) |
| O10-C35 | 1.271(6) | C13-N3-C15 | 112.8(3) |
| O1-C7 | 1.356(5) | O2-N2-C13 | 125.4(4) |
| O1-C6 | 1.414(6) | O2-N2-C14 | 120.1(3) |