Chemical formula

C16H30Mn2N10O6·4(Cl) (1)

C7H13CoN6O6·NO3(2)

Mr

710.18

398.16

Crystal system

Triclinic

Triclinic

Space group

P-1

P-1

Temperature (K)

293

293

a (Å)

8.7932 (2)

8.4248 (2)

b (Å)

9.1070 (2)

8.7674 (2)

c (Å)

9.9348 (3)

10.6885 (2)

α (˚)

75.460 (2)

82.151 (2)

β (˚)

67.174 (2)

86.273 (2)

γ (˚)

81.729 (2)

81.732 (2)

V (Å3)

708.83 (3)

773.14 (3)

Z

1

2

Radiation type

Mo Kα

Mo Kα

µ (mm−1)

1.32

1.17

Crystal size (mm)

0.40 × 0.30 × 0.15

0.34 × 0.22 × 0.10

Tmin, Tmax

0.574, 1.000

0.763, 1.000

No. of measured reflections

15348

29332

Independent reflections

3394

3611

Observed reflections [I > 2σ(I)]

3030

3296

Rint

0.048

0.027

R[F2 > 2σ(F2)]

0.026

0.045

wR(F2)

0.069

0.130

Data/parameters/restraints

3389/192/5

3611/269/0

GOF

1.07

1.07

Δρmax, Δρmin (e∙Å−3)

0.28, −0.28

1.00, −0.57