Chemical formula | C16H30Mn2N10O6·4(Cl) (1) | C7H13CoN6O6·NO3(2) |
Mr | 710.18 | 398.16 |
Crystal system | Triclinic | Triclinic |
Space group | P-1 | P-1 |
Temperature (K) | 293 | 293 |
a (Å) | 8.7932 (2) | 8.4248 (2) |
b (Å) | 9.1070 (2) | 8.7674 (2) |
c (Å) | 9.9348 (3) | 10.6885 (2) |
α (˚) | 75.460 (2) | 82.151 (2) |
β (˚) | 67.174 (2) | 86.273 (2) |
γ (˚) | 81.729 (2) | 81.732 (2) |
V (Å3) | 708.83 (3) | 773.14 (3) |
Z | 1 | 2 |
Radiation type | Mo Kα | Mo Kα |
µ (mm−1) | 1.32 | 1.17 |
Crystal size (mm) | 0.40 × 0.30 × 0.15 | 0.34 × 0.22 × 0.10 |
Tmin, Tmax | 0.574, 1.000 | 0.763, 1.000 |
No. of measured reflections | 15348 | 29332 |
Independent reflections | 3394 | 3611 |
Observed reflections [I > 2σ(I)] | 3030 | 3296 |
Rint | 0.048 | 0.027 |
R[F2 > 2σ(F2)] | 0.026 | 0.045 |
wR(F2) | 0.069 | 0.130 |
Data/parameters/restraints | 3389/192/5 | 3611/269/0 |
GOF | 1.07 | 1.07 |
Δρmax, Δρmin (e∙Å−3) | 0.28, −0.28 | 1.00, −0.57 |