No. | Compounds | Formula | Тmelt. ˚C | Output % | Rf | Calculated % (found %) elemental compositions | |||
С | H | N | S | ||||||
20 | N-methyl-N1-(β-D-xylopyranosyl)-thiourea | С7Н14N2O4S | 122 - 125 | 53 | 0.2 | 37.82 (37.97) | 6.34 (6.45) | 12.60 (12.80) | 14.42 (14.60) |
21 | N-methyl-N1-(β-D-galactopyranosyl)-thiourea | С8Н16N2O5S | 168 - 170 | 48 | 0.8 | 38.08 (38.25) | 6.39 (6.50) | 11.10 (11.29) | 12.71 (12.85) |
22 | N-methyl-N1-(β-D-glucopyranosyl)-thiourea | С8Н16N2O5S | 165 - 167 | 58 | 0.6 | 38.08 (38.24) | 6.39 (6.50) | 11.10 (11.25) | 12.71 (12.87) |
23 | N-(β-D-xylopyranosyl) phenylthiosemicarbazide | С12Н17N3O4S | 149 - 152 | 52 | 0.87 | 48.14 (48.04) | 5.72 (5.98) | 14.03 (13.94) | 10.71 (10.86) |
24 | N-(β-Dgalactopyranosyl) phenylthiosemicarbazide | С13Н19N3O5S | 137 - 140 | 56 | 0.84 | 47.40 (47.21) | 5.81 (5.98) | 12.75 (12.94) | 9.73 (9.45) |
25 | N-(β-D-glucopyranosyl) -phenylthiosemicarbazide | С13Н19N3O5S | 142 - 144 | 55 | 0.75 | 47.40 (47.23) | 5.81 (6.05) | 12.75 (12.92) | 9.73 (9.94) |
26 | 1-[(N-β-xylopyranosyl)-thiocarbamoyl] -3,5-dimethylpyrazole | С11Н17N3O4S | 116 - 117 | 58 | 0.89 | 45.98 (46.07) | 5.96 (6.13) | 14.62 (14.80) | 11.15 (11.25) |
27 | 1-[(N-β-galactopyranosyl)-thiocarbamoyl] -3,5-dimethylpyrazole | С12Н19N3O5S | 146 - 148 | 61 | 0.6 | 45.41 (45.67) | 6.03 (6.15) | 13.24 (13.40) | 10.10 (10.25) |
28 | 1-[(N-β-glucopyranosyl)-thiocarbamoyl] -3,5-dimethylpyrazole | С12Н19N3O5S | 150 - 151 | 56.5 | 0.7 | 45.41 (45.52) | 6.03 (5.96) | 13.24 (13.45) | 10.10 (10.35) |
29 | 4-(N-β-D-xylopyranosyl)thiosemicarbazide | С6Н13N3O4S | 217 - 219 | 35.6 | 0.8 | 32.28 (32.40) | 5.86 (6.10) | 18.82 (18.97) | 14.36 (14.47) |
30 | 4-(N-β-D-galactopyranosyl)thiosemicarbazide | С7Н15N3O5S | 210 - 211 | 46 | 0.9 | 33.19 (33.36) | 5.96 (6.28) | 16.59 (16.75) | 12.65 (12.98) |
31 | 4-(N-β-D-glucopyranosyl)thiosemicarbazide | С7Н15N3O5S | 205 - 206 | 37 | 0.6 | 33.19 (33.32) | 5.96 (6.26) | 16.59 (16.64) | 12.65 (12.85) |
32 | 2,3,4,6-tetra-О-acetyl-(β-D-glycopyranosyl) -thiocarbamoyl diethylene diamine) | С22Н35N3O9S | 135 - 137 | 62.5 | 0.84 | 51.05 (50.97) | 6.81 (6.98) | 8.11 (8.33) | 6.19 (6.35) |