Bond Angle (˚) |
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C1-N1-C2 | 108.5 (3) | O1-C1-O2 | 123.8 (4) | |||||
O1-C1-N1 | 130.7 (4) | O2-C1-N1 | 105.4 (3) | |||||
C1-O2-N2 | 109.8 (3) | C2-N2-O2 | 103.8 (3) | |||||
N2-C2-N1 | 112.4 (3) | N2-C2-C3 | 124.2 (3) | |||||
N1-C2-C3 | 123.4 (3) | C16-N3-C22 | 105.5 (3) | |||||
C16-N3-C15 | 123.5 (3) | C22-N3-C15 | 131.1 (3) | |||||
C16-N4-C17 | 103.0 (3) | N3-C15-C12 | 114.0 (3) | |||||
C16-O5-C24 | 118.2 (3) | N4-C16-N3 | 115.9 (3) | |||||
N4-C16-O5 | 128.3 (3) | C18-C17-N4 | 128.1 (3) | |||||
O5-C16-N3 | 115.9 (3) | N3-C22-C21 | 134.0 (3) | |||||
N4-C17-C22 | 110.9 (3) | O3-C23-O4 | 122.7 (4) | |||||
N3-C22-C17 | 104.8 (3) | O4-C23-C21 | 114.3 (3) | |||||
O3-C23-C21 | 123.0 (3) | O5-C24-C25 | 106.9 (3) | |||||
Dihedral Angles (˚) |
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Crystal: Ring | I | II | III | IV | V | |||
I O(2)N(2)C(2)N(1)C(1) |
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II N(3)C(16)N(4)C(17)C(22) | 35.9 (2) |
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III C(3)C(4)C(5)C(6)C(7)C(8) | 71.9 (2) | 47.1 (2) |
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IV C(9)C(10)C(11)C(12)C(13)C(14) | 76.7 (2) | 68.2 (2) | 60.04 (19) |
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V C(17)C(18)C(19)C(20)C(21)C(22) | 38.05 (19) | 2.33 (19) | 46.78 (18) | 65.93 (18) |
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VI N(3)C(16)N(4)C(17)C(18)C(19)C(20)C(21)C(22) | 37.11 (17) | 1.28 (17) | 46.87 (16) | 66.94 (16) | 1.05 (15) | |||