| Compound | Retention time (min) | Precursor ion (m/z) | MRM 1 (quantification) (m/z) | MRM 2 (confirmation) (m/z) | Fragmentor (V) | Collision energy (V) |
| MeP | 6.225 | 151.2 | 92.1 | 136.1 | 70 | 16 |
| EtP | 9.006 | 165.2 | 92.1 | 137.1 | 79 | 20 |
| PrP | 11.578 | 179.2 | 92.1 | 136.1 | 99 | 24 |
| PFBuA | 3.322 | 213 | 169 | 51.6 | 55 | 0 |
| PFPeA | 7.302 | 263 | 219 | 89.7 | 55 | 0 |
| PFHxA | 10.453 | 313 | 269 | 119 | 60 | 0 |
| PFHpA | 12.647 | 363.1 | 319 | 332.8 | 65 | 0 |
| PFOA | 14.268 | 413.1 | 369.1 | 194.3 | 62 | 0 |
| PFOS | 15.595 | 499 | 80 | 51.5 | 145 | 40 |
| HBCDD | 21.918 | 640.7 | 81 | 79 | 67 | 40 |