| Bath composition | mol/dm3 |
| FeSO4∙7H2O | 0.050 |
| NiSO4∙6H2O | 0.099 |
| H3BO3 | 0.243 |
| C2H8O7 | 0.026 |
| Plating Conditions | |
| Current density | 25 mA/dm2 |
| Plating period | 20 min |
| Bath temperature | 40˚C |
| pH | 2.50 |
| Counter electrode | Ni plate |