LC-MS/MS

SHIMADZU LCMS/MS-8040.

Detector

Mass Spectrophotometer

Column

Kinetex, 2.6 µ, C18 Column, 100 × 3.0.

Column oven temperature

40˚C

Retention time

Fluopyram Benzamide―1.5 min

Nebulizing gas

Nitrogen

Nebulizing gas flow

2.0 litres/min

Pump mode/flow

Gradient/0.4 ml/min

LC programme

A: Ammonium Formate in Water (10 Mm)―40%

B: Ammonium Formate in Methanol (10 Mm)―60%

LC programme

Time solvent Conc.

0.01 B Conc. 50%

2.00 B Conc. 80%

3.00 B Conc. 50%

4.00 B Conc. 50%

Total time programme

4 min