Ratio(NFX-GLU) | solvent | crystallization | suitable for SCXRD |
1:1 | H2O | × | × |
1:1 | H2O-CH3OH(1:1) | × | × |
1:1 | H2O-CH3OH(1:3) | √ | × |
1:1 | H2O-C2H5OH(1:3) | √ | × |
2:1 | H2O | × | × |
2:1 | H2O-CH3OH(1:1) | × | × |
2:1 | H2O-CH3OH(1:3) | √ | × |
2:1 | H2O-C2H5OH(1:3) | √ | × |
1:2 | H2O | × | × |
1:2 | H2O-CH3OH(1:1) | × | × |
1:2 | H2O-CH3OH(1:3) | √ | × |
1:2 | H2O-C2H5OH(1:3) | √ | × |
1:2 | H2O-CH3CN-CH3OH(1:2:1) | √ | √ |
1:2 | H2O-CH3CN-CH3OH(2:1:1) | × | × |
1:2 | H2O-CH3CN-CH3OH(1:1:2) | × | × |