40 | White porcelanaceous fragments, conchoidal fracture. | Silicon, aluminum and oxygen | Beryl ICDD PDF 84-1141 | Beryl, Be3Al2Si6O18 EDS did not determine the presence of beryllium, due to its low atomic mass |
41 | Dark, blackish fragments with conchoidal fractures | Oxygen, aluminum, calcium, iron and silicon, REE elements (La, Ce, Nd) | The spectrum is probably matching the Allanite’s one | Allanite (epidote group) (Ca,REE)2(Fe,Al)3(SiO4)3(OH) XRPD spectrum shows a low crystallinity, probably due to a radiation damage (metamictization) of the crystalline structure |
42 | Yellow and dark yellow fragments, no cleavage, conchoidal fracture | Oxygen, silicon and zirconium | Zircon ICDD PDF 83-1375 | Zircon, ZrSiO4 |
43 | Blackish, dark fragments with no distinctive features | Oxygen, carbon, fluorine and REE elements (La, Ce, Nd) | Parasite ICDD PDF 47-1832 and Bastnaesite ICDD PDF 11-0340 | Bastnaesite, CeCO3F Parisite, Ca(Ce,La)2F2(CO3)3 Probably a natural blend of the two minerals, used as standard for REE carbonates. |
44 | Greyish-green fragments | Phosphor, oxygen, thorium, calcium, REE elements (Ce, La, Nd) | Neodymium phosphate ICDD PDF 83-0654 | Monazite, (Ce,REE)PO4 |
45 | Black fragments | Manganese, sulphur | Alabandite ICDD PDF 88-2223 | Alabandite, (MnS) |
46 | Black fragments, with fibrous appearance. Black streak | Manganese and oxygen | Pyrolusite ICDD PDF 72-1984 | Pyrolusite, MnO2 |
47 | Pink fragments with cleavage traces, low hardness | Manganese, oxygen, carbon and a minor amount of calcium | Rhodochrosite ICDD PDF 44-1472 | Rhodochrosite, MnCO3 |
48 | Pink fragments without any cleavage | Silicon, oxygen, manganese and minor amount of calcium and magnesium | Rhodonite ICDD PDF 83-2212 and Bustamite ICDD PDF 85-1034 | Rhodonite (magnesian), (Mn,Mg)SiO3 Bustamite, (Ca,Mn)SiO3 Probably a natural mix of the two Mn-rich silicates Rhodonite and Bustamite |
49 | Sand | Oxygen, silicon, sodium, potassium and calcium | Quartz ICDD PDF 86-1629 and Albite ICDD PDF 09-0466 | Quartz, sodic feldspar, potassic feldspar Sand, mainly composed of Quartz and Feldspars. |
50 | Intense yellow fragments, vitreous, with some cleavage | Zinc, sulphur and iron | Pyrrothite ICDD PDF 76-2308 and Sphalerite ICDD PDF 77-2100 | Pyrrothite (Fe7S8) Sphalerite (ZnS) A mix of iron and zinc sulphides |
51 | Pale yellowish powder, with some metallic lustre | Iron, sulphur and oxygen | Pyrite ICDD PDF 89-3057 | Pyrite, FeS2 The sample was probably made of crushed Pyrite, strongly oxidized during a century. |
52 | Black fragments | Mainly iron and oxygen, some aluminum and calcium in small portions | Magnetite ICDD PDF 88-0315 | Magnetite, Fe3O4 Impurities of silicates |
53 | Dark reddish fragments with fibrous appearance | Iron and oxygen, minor amount of aluminum and silicon | Hematite ICDD PDF 89-0599 | Hematite, Fe2O3 |
54 | Reddish-yellowish dark fragments, fibrous appearance | Oxygen and iron | Goethite ICDD PDF 29-0713 | Goethite, FeO(OH) |
55 | Rhombohedrical shaped fragment, dark yellow | Iron, oxygen and carbon | Siderite ICDD PDF 83-1764 | Siderite, FeCO3 |
56 | Grey-greenish fragments with conchoidal fracture | Iron, phosphor, oxygen and minor amount of sodium, aluminium. | Natrodufrenite ICDD PDF 35-0570 | Vivianite, Fe3(PO4)2・8H2O The sample was probably vivianite, altered in Natrodufrenite |