Treatment

run

Time of reaction

(x₁, min)

Temperature

(x₂, ˚C)

NaOCH₃

(x₃, % w/w)

PEG400

(x₄, % w/w)

1

150

160

2

1.5

2^c

210

140

3

1.0

3

150

160

4

0.5

4

150

120

2

0.5

5

270

160

2

0.5

6

270

120

2

1.5

7

150

120

4

1.5

8

270

120

4

0.5

9

270

160

4

1.5

10^c

210

140

3

1.0

11

210

140

5

1.0

12

210

140

1

1.0

13

330

140

3

1.0

14

90

140

3

1.0

15

210

140

3

0.0

16

210

180

3

1.0

17

210

140

3

2.0

18^c

210

140

3

1.0

19

210

100

3

1.0

20^c

210

140

3

1.0

21

270

160

2

1.5

22^c

210

140

3

1.0

23

150

160

2

0.5

24

150

120

4

0.5

25^c

210

140

3

1.0

26

270

160

4

0.5

27

150

160

4

1.5

28

270

120

2

0.5

29

270

120

4

1.5

30

150

120

2

1.5