Amount spiked*

% of Recovery†

TAM

SOL

TAM-1

TAM-2

TAM-3

TAM-4

SOL-1

SOL-2

SOL-3

LOQ

98.8 ± 2.5

98.7 ± 3.1

98.8± 2.3

99.3 ± 2.2

98.9 ± 0.6

99.6 ± 1.8

100.0 ± 3.3

101.0 ± 2.6

100.9 ± 2.1

50%

99.4 ± 1.0

99.6 ± 1.0

99.1 ± 0.2

99.5 ± 0.5

99.4 ± 1.5

100.1 ± 0.9

101.3 ± 2.1

101.2 ± 0.4

101.0 ±0.5

100%

100.2 ± 0.4

99.4 ± 2.0

100.4 ± 0.7

100.0 ± 1.1

100.3 ± 0.7

100.1 ± 1.3

99.9 ± 0.6

101.3 ± 0.6

100.2 ± 0.7

150%

98.9 ± 2.3

99.0 ± 0.4

100.0 ± 0.9

100.7 ± 0.8

99.7 ± 1.3

101.0 ± 1.4

100.2 ± 0.5

100.6 ± 1.6

101.2 ± 0.8

200%

98.6 ± 2.5

100.6 ± 0.7

99.8 ± 0.3

100.3 ± 0.7

100.6 ± 0.3

99.9 ± 1.3

99.9 ± 0.4

101.8 ± 0.4

100.8 ± 1.1