Component

Recovery results (Mean % Recoverya ± %RSD)

LOQ level; amount (%w/w)

50% of specification levelb; amount (%w/w)

100% of specification levelb; amount (%w/w)

150% of specification levelb; amount (%w/w)

Imp-1

103.33 ± 0.19

100.00 ± 0.64

96.08 ± 1.19

92.14 ± 1.55

Imp-2

105.11 ± 0.58

101.32 ± 1.54

100.66 ± 0.89

100.44 ± 1.97

Imp-3

106.67 ± 1.99

103.95 ± 0.91

101.96 ± 0.66

101.75 ± 0.97

Imp-4

113.33 ± 2.14

103.95 ± 0.81

101.32 ± 0.87

99.56 ± 0.96

Imp-5

103.33 ± 1.21

100.00 ± 1.99

101.21 ± 1.14

98.25 ± 2.57

Imp-6

110.00 ± 1.56

103.95 ± 0.72

101.32 ± 0.37

104.23 ± 0.59

Imp-7

116.67 ± 2.11

101.21 ± 1.64

100.54 ± 1.89

102.11 ± 0.21

Imp-8

95.26 ± 2.11

96.54 ± 2.41

97.05 ± 1.05

95.11 ± 1.14