Temperature (˚C)

pH Value

3 h

6 h

9 h

12 h

4

3

1.9 - 5.9 nm

1.7 - 7.2 nm

2.1 - 9.2 nm

3.7 - 28.3 nm

Unmodified (6.5)

2.0 - 8.2 nm

3.4 - 10.3 nm

3.3 - 40.2 nm

7.5 - 110.3 nm

10

3.5 - 10.4 nm

2.1 - 6.8 nm

5.9 - 15.8 nm

10.0 - 41.3 nm

25

3

2.1 - 20.1 nm

2.5 - 24.0 nm

2.5 - 25.0 nm

2.1 - 19.9 nm

Unmodified (6.5)

1.7 - 22.5 nm

2.5 - 17.4 nm

1.9 - 21.0 nm

1.9 - 19.5 nm

10

1.0 - 22.5 nm

1.7 - 21.5 nm

2.1 - 21.7 nm

1.4 - 21.0 nm

37

3

7.1 - 43.1 nm

6.5 - 36.5 nm

3.3 - 34.3 nm

4.3 - 62.8 nm

Unmodified (6.5)

3.3 - 59.9 nm

3.2 - 21.9 nm

2.3 - 32.0 nm

2.9 - 26.3 nm

10

7.5 - 96.5 nm

4.4 - 148.0 nm

2.5 - 44.3 nm

2.9 - 44.9 nm

60

3

11.6 - 330.8 nm

1.8 - 308.7 nm

2.1 - 12.3 nm

1.4 - 88.7 nm

Unmodified (6.5)

3.6 - 44.7 nm

4.1 - 46.1 nm

2.7 - 36.2 nm

4.3 - 124.9 nm

10

4.2 - 47.9 nm

1.4 - 93.6 nm

1.4 - 73.8 nm

1.8 - 8.1 nm

80

3

11.6 - 330.8 nm

1.8 - 308.7 nm

2.1 - 12.3 nm

1.4 - 88.7 nm

Unmodified (6.5)

2.4 - 20.5 nm

4.3 - 101.0 nm

2.7 - 23.9 nm

2.7 - 20.5 nm

10

1.9 - 15.4 nm

2.4 - 35.4 nm

2.4 - 12.4 nm

17.2 - 409.4 nm