Temperature, ˚C/time

1 min

3 min

9 min

27 min

81 min

72 h

T-C, equilibrium

975

0

0

0

0

0

0.6 ± 0.3

0

950

0

0

0

0

0

15.6 ± 1.6

0

900

0.1 ± 0.1

0.1 ± 0.1

0.9 ± 0.5

4.0 ± 0.9

14.2 ± 1.7

32.5 ± 1.8

0

850

0

0.2 ± 0.2

3.4 ± 0.9

14.8 ± 1.4

24.9 ± 1.7

36.1 ± 2.0

0

800

0

0.2 ± 0.2

1.1 ± 0.4

9.2 ± 1.4

28.0 ± 1.8

37.5 ± 2.0

10.6

750

0

0

0

1.7 ± 0.6

29.6 ± 1.9

37.6 ± 1.9

24.5

700

0

0

0

0

0.5 ± 0.3

42.3 ± 2.4

31.1