Experiment

Temperature (˚C)

Sample volume (mL)

Solvent volume (mL)

1

70 (−)

5 (−)

5 (−)

2

110 (+)

5 (−)

5 (−)

3

70 (−)

10 (+)

5 (−)

4

110 (+)

10 (+)

5 (−)

5

70 (−)

5 (−)

10 (+)

6

110 (+)

5 (−)

10 (+)

7

70 (−)

10 (+)

10 (+)

8

110 (+)

10 (+)

10 (+)