Experiment | Temperature (˚C) | Sample volume (mL) | Solvent volume (mL) |
1 | 70 (−) | 5 (−) | 5 (−) |
2 | 110 (+) | 5 (−) | 5 (−) |
3 | 70 (−) | 10 (+) | 5 (−) |
4 | 110 (+) | 10 (+) | 5 (−) |
5 | 70 (−) | 5 (−) | 10 (+) |
6 | 110 (+) | 5 (−) | 10 (+) |
7 | 70 (−) | 10 (+) | 10 (+) |
8 | 110 (+) | 10 (+) | 10 (+) |