Injection

Splitless (1 min)

Injector temperature

250˚C

Column temperature

80˚C

Flow

He, 1.0 mL∙min⁻¹

Oven temperature program

50˚C∙min⁻¹ up to 100˚C

+ 15˚C∙min⁻¹ up to 230˚C (3:00 min)

+ 5˚C∙min⁻¹ up to 270˚C