Atom

Gossypetin (8)

Gossypetin (10)

Gossypitrin (10)

Cuba sample*

13C (ppm)

13C (ppm)

13C (ppm)

13C (ppm)

1H (ppm)

M

I

J (Hz)

1

/

/

/

/

/

2

146.5

146.7

147.8

145.8

/

3

135.3

135.5

136.1

135.6

/

4

175.9

176.6

176.6

176.06

/

4a

102.6

103.8

104.9

102.62

/

5

152.1

152.7

151.7

152.3

/

6

97.8

98.0

98.1

97.98

6.25

s

1

/

7

152.5

152.3

150.6

153.08

/

8

124.6

124.7

127.1

124.3

/

8a

144.76

144.9

143.8

144.9

/

1’

122.2

122.3

122.4

122.3

/

2’

115.2

115.3

115.5

115.79

8.07

d

1

2.02

3’

144.85

145.0

145.4

144.9

/

4’

147.5

147.7

148.2

148.6

/

5’

115.3

115.5

115.9

115.86

6.99

d

1

8.71

6’

120.1

120.3

120.6

123.28

7.92

d

1

8.71

1’’

101.6

101.84

4.83

d

1

7.32

2’’

73.5

73.12

3.44-3.34

m

1

**

3’’

77.5

75.97

3.44-3.34

m

1

**

4’’

70.0

69.14

3.44-3.34

m

1

**

5’’

76.0

76.72

3.44-3.34

m

1

**

6’’

61.0

60.15

3.76

d

1

11.82

3.63

dd

1

11.82

3.58