Results | |||||||||
Run no | Experimental design | Experimental | Predicted | ||||||
Monomer ratio (%) A | Particle size (µm) B | Initiator conc. (%) C | Density (g/cm3) | Homopolymer (g) | Grafting efficiency | % swelling | Grafting efficiency | % swelling | |
1 | 5 | 1000.00 | 0.50 | 0.075 | 0.021 | 8.78 | 637.20 | 8.013 | 675.74 |
2 | 5 | 125.00 | 2.50 | 0.068 | 0.049 | 24.18 | 326.30 | 23.32 | 312.75 |
3 | 12.5 | 562.50 | 1.50 | 0.088 | 0.036 | 4.47 | 474.30 | 5.36 | 383.75 |
4 | 20 | 125.00 | 0.50 | 0.106 | 0.027 | 14.63 | 342.90 | 16.07 | 307.71 |
5 | 5 | 125.00 | 0.50 | 0.140 | 0.004 | 11.70 | 305.00 | 15.41 | 322.16 |
6 | 20 | 125.00 | 2.50 | 0.120 | 0.026 | 15.18 | 453.90 | 16.61 | 415.70 |
7 | 5 | 1000.00 | 2.50 | 0.058 | 0.054 | 13.57 | 365.10 | 12.79 | 400.63 |
8 | 12.5 | 562.50 | 1.50 | 0.072 | 0.045 | 4.67 | 365.10 | 5.36 | 383.75 |
9 | 12.5 | 562.50 | 0.50 | 0.078 | 0.012 | 11.52 | 516.70 | 5.71 | 482.30 |
10 | 12.5 | 562.50 | 1.50 | 0.071 | 0.058 | 4.67 | 365.10 | 5.36 | 383.75 |
11 | 12.5 | 562.50 | 2.50 | 0.102 | 0.010 | 4.99 | 365.70 | 8.36 | 398.74 |
12 | 20 | 1000.00 | 2.50 | 0.074 | 0.001 | 3.69 | 389.70 | 0.70 | 372.88 |
13 | 12.5 | 1000.00 | 1.50 | 0.085 | 0.019 | 2.29 | 501.70 | 5.53 | 430.56 |
14 | 12.5 | 562.50 | 1.50 | 0.083 | 0.042 | 4.57 | 365.10 | 5.36 | 383.75 |
15 | 12.5 | 125.00 | 1.50 | 0.079 | 0.034 | 22.86 | 205.40 | 17.18 | 275.18 |
16 | 20 | 562.50 | 1.50 | 0.074 | 0.022 | 2.72 | 304.50 | 1.51 | 380.82 |
17 | 12.5 | 562.50 | 1.50 | 0.083 | 0.042 | 4.17 | 365.10 | 5.36 | 383.75 |
18 | 20 | 1000.00 | 0.50 | 0.075 | 0.032 | 1.72 | 516.70 | 3.30 | 530.59 |
19 | 12.5 | 562.50 | 1.50 | 0.083 | 0.042 | 4.37 | 365.10 | 5.36 | 383.75 |
20 | 5 | 562.50 | 1.50 | 0.073 | 0.044 | 8.45 | 479.60 | 7.22 | 401.92 |