Dispersed water phase

Distilled Water

5.0 g

Erythritol

5.0 g

PEG

0.5 - 6.0 g (9.0 wt% - 55 wt% H2O)

Oil phase

Corn Oil

98.5 g

Poem PR-100

1.5 g (1 wt% oil phase)

Additional phase

Corn Oil

72.0 g

Poem PR-100

0.79 g (1 wt% oil phase)

Isocyanete (TDI, MDI, HDI)

6.0 g (3.36 wt% oil phase)

Pouring Velocity

150 ml/min

Formation of (w/o) emulsion

Time

10 min

Impeller speed

300 rpm

Temperature

70˚C

Interfacial Polycondensation

Time

24 h

Impeller speed

300 rpm

Temperature

70˚C

Supercooling prevention agent

Calcium Sulfate

Calcium Phosphate