Soaking time

I

II

III

Slope

R2b

LRa, M

DL, M

Slope

R2b

LRa, M

DL, M

Slope

R2b

LRa, M

DL, M

1 day

59

0.999

10-2 - 2.5 × 10−5

2.0 × 10−5

15

1

10−2 - 1.5 × 10−5

3.1 × 10−7

30

0.999

10−2 - 2.5 × 10−5

1.2 × 10−5

6 days

48

1

10−2 - 2.5 × 10−5

1.5 × 10−5

32

1

10−2 - 1.5 × 10−5

6.3 × 10−6

22

0.993

10−2 - 3.9 × 10−5

1.2 × 10−5

8 days

38.5

0.948

10−2 - 2.5 × 10−6

10−6

39

0.999

10−2 - 2.5 × 10−5

1 × 10−5

24

1

10−2 - 2.5 × 10−5

5.0 × 10−6

42 days

36.5

0.9895

10−2 - 1.5 × 10−6

6.3 × 10−7

32

0.9987

10−2 - 1.0 × 10−5

2.5 × 10−6

25

0.9586

10−2 - 2.5 × 10−5

5.0 × 10−6

2 months

39

0.992

10−2 - 1 × 10−5

3.9 × 10−6

47

0.999

10−2 - 6.3 × 10−5

1.5 × 10−5

25.5

0.999

10−2 - 3.9 × 10−5

3.9 × 10−6