Run | Temperature (K) | Acid conc.(M) | S/L ratio (g/ml) | Stirring rate (rpm) | Time (min) | Yield (%) |
1 | 338 | 2.75 | 0.03 | 385 | 90 | 83.8 |
2 | 353 | 1.5 | 0.04 | 540 | 60 | 70.8 |
3 | 353 | 4 | 0.04 | 230 | 60 | 68.6 |
4 | 338 | 2.75 | 0.03 | 695 | 90 | 82.3 |
5 | 323 | 4 | 0.04 | 230 | 120 | 69.6 |
6 | 353 | 4 | 0.02 | 540 | 60 | 82.8 |
7 | 353 | 4 | 0.04 | 540 | 120 | 81.8 |
8 | 323 | 4 | 0.02 | 230 | 60 | 68.5 |
9 | 338 | 0.25 | 0.03 | 385 | 90 | 67.6 |
10 | 323 | 1.5 | 0.02 | 230 | 120 | 70.1 |
11 | 368 | 2.75 | 0.03 | 385 | 90 | 82.5 |
12 | 338 | 2.75 | 0.03 | 385 | 90 | 84.2 |
13 | 338 | 2.75 | 0.03 | 385 | 30 | 68.7 |
14 | 338 | 2.75 | 0.03 | 385 | 90 | 84.8 |
15 | 353 | 1.5 | 0.02 | 230 | 60 | 69.5 |
16 | 338 | 2.75 | 0.03 | 75 | 90 | 67.8 |
17 | 323 | 4 | 0.02 | 540 | 120 | 81.7 |
18 | 308 | 2.75 | 0.03 | 385 | 90 | 67.8 |
19 | 338 | 2.75 | 0.05 | 385 | 90 | 67.7 |
20 | 353 | 4 | 0.02 | 230 | 120 | 81.6 |
21 | 338 | 2.75 | 0.03 | 385 | 90 | 82.7 |
22 | 353 | 1.5 | 0.04 | 230 | 120 | 69.6 |
23 | 338 | 2.75 | 0.03 | 385 | 90 | 82.2 |
24 | 323 | 1.5 | 0.04 | 230 | 60 | 52.3 |
25 | 338 | 5.25 | 0.03 | 385 | 90 | 82.6 |
26 | 353 | 1.5 | 0.02 | 540 | 120 | 81.7 |
27 | 338 | 2.75 | 0.03 | 385 | 90 | 82.3 |
28 | 338 | 2.75 | 0.03 | 385 | 150 | 83.8 |
29 | 323 | 1.5 | 0.04 | 540 | 120 | 69.5 |
30 | 338 | 2.75 | 0.01 | 385 | 90 | 83.9 |
31 | 323 | 1.5 | 0.02 | 540 | 60 | 70.6 |
32 | 323 | 4 | 0.04 | 540 | 60 | 70.9 |