NDMA | NMEA | NDEA | NPIP | NPYR | NMOR | |
Pipette Mixing―8 loops | 58.3 (+1.6%) | 46.5 (+5.0%) | 44.2 (+0.9%) | 40.8 (+0.5%) | 64.5 (+4.9%) | 52.9 (+2.7%) |
Pipette Mixing―10 loops* | 57.4 | 44.3 | 43.8 | 40.6 | 61.5 | 51.5 |
Pipette Mixing―12 loops | 58.9 (+2.6%) | 46.8 (+5.6%) | 47.0 (+7.3%) | 43.6 (+7.4%) | 61.9 (+0.7%) | 52.7 (+2.3%) |
DCM volume―2 mL | 60.1 (−1.2%) | 46.0 (−2.1%) | 46.5 (−0.6%) | 41.4 (−4.6%) | 62.9 (−0.8%) | 57.9 (+5.5%) |
DCM volume―2.5 mL* | 60.8 | 47.0 | 46.8 | 43.4 | 63.4 | 54.9 |
DCM volume―3 mL | 59.8 (−1.6%) | 38.4 (−18.3%) | 42.0 (-10.3%) | 35.7 (−17.7%) | 56.3 (−11.2%) | 44.0 (−19.9%) |
Injection volume―4 µL | 69.0 (−5.2%) | 46.6 (+2.0%) | 51.3 (+1.6%) | 44.1 (+1.4%) | 60.6 (−5.6%) | 53.8 (−2.0%) |
Injection volume―5 µL* | 72.8 | 45.7 | 50.5 | 43.5 | 64.2 | 54.9 |
Injection volume―6 µL | 76.8 (+5.5%) | 46.4 (+1.5%) | 50.8 (+0.6%) | 44.1 (+1.4%) | 63.6 (−0.9%) | 53.1 (−3.3%) |
Source temperature―225˚C | 69.8 (−7.9%) | 46.7 (+1.7%) | 50.2 (−2.1%) | 42.4 (−3.9%) | 62.5 (−2.6%) | 52.2 (−1.1%) |
Source temperature―250˚C* | 75.8 | 45.9 | 51.3 | 44.1 | 64.2 | 52.8 |
Source temperature―275˚C | 85.0 (+12.1%) | 47.9 (+4.4%) | 51.9 (+1.2%) | 46.6 (+5.7%) | 63.8 (−0.6%) | 53.8 (+1.9%) |
CI gas―20% | 62.5 (−3.1%) | 40.7 (+3.3%) | 43.5 (−1.4%) | 37.5 (+1.4%) | 58.2 (+2.3%) | 48.4 (+1.7%) |
CI gas―25%* | 64.5 | 39.4 | 44.1 | 37.0 | 56.9 | 47.6 |
CI gas―30% | 74.6 (+15.7%) | 40.7 (+3.3%) | 43.2 (−2.0%) | 35.8 (−3.2%) | 57.5 (+1.0%) | 45.9 (−3.6%) |