NDMA

NMEA

NDEA

NPIP

NPYR

NMOR

Pipette Mixing―8 loops

58.3 (+1.6%)

46.5 (+5.0%)

44.2 (+0.9%)

40.8 (+0.5%)

64.5 (+4.9%)

52.9 (+2.7%)

Pipette Mixing―10 loops*

57.4

44.3

43.8

40.6

61.5

51.5

Pipette Mixing―12 loops

58.9 (+2.6%)

46.8 (+5.6%)

47.0 (+7.3%)

43.6 (+7.4%)

61.9 (+0.7%)

52.7 (+2.3%)

DCM volume―2 mL

60.1 (−1.2%)

46.0 (−2.1%)

46.5 (−0.6%)

41.4 (−4.6%)

62.9 (−0.8%)

57.9 (+5.5%)

DCM volume―2.5 mL*

60.8

47.0

46.8

43.4

63.4

54.9

DCM volume―3 mL

59.8 (−1.6%)

38.4 (−18.3%)

42.0 (-10.3%)

35.7 (−17.7%)

56.3 (−11.2%)

44.0 (−19.9%)

Injection volume―4 µL

69.0 (−5.2%)

46.6 (+2.0%)

51.3 (+1.6%)

44.1 (+1.4%)

60.6 (−5.6%)

53.8 (−2.0%)

Injection volume―5 µL*

72.8

45.7

50.5

43.5

64.2

54.9

Injection volume―6 µL

76.8 (+5.5%)

46.4 (+1.5%)

50.8 (+0.6%)

44.1 (+1.4%)

63.6 (−0.9%)

53.1 (−3.3%)

Source temperature―225˚C

69.8 (−7.9%)

46.7 (+1.7%)

50.2 (−2.1%)

42.4 (−3.9%)

62.5 (−2.6%)

52.2 (−1.1%)

Source temperature―250˚C*

75.8

45.9

51.3

44.1

64.2

52.8

Source temperature―275˚C

85.0 (+12.1%)

47.9 (+4.4%)

51.9 (+1.2%)

46.6 (+5.7%)

63.8 (−0.6%)

53.8 (+1.9%)

CI gas―20%

62.5 (−3.1%)

40.7 (+3.3%)

43.5 (−1.4%)

37.5 (+1.4%)

58.2 (+2.3%)

48.4 (+1.7%)

CI gas―25%*

64.5

39.4

44.1

37.0

56.9

47.6

CI gas―30%

74.6 (+15.7%)

40.7 (+3.3%)

43.2 (−2.0%)

35.8 (−3.2%)

57.5 (+1.0%)

45.9 (−3.6%)