Reaction temperature (˚C) | Color | Reaction time (h) | Yield (%) |
90 | White | 4.0 | 22.1 |
95 | White | 4.0 | 30.5 |
100 | White | 4.0 | 65.0 |
105 | Faint yellow | 4.0 | 98.0 |
110 | Faint yellow | 4.0 | 98.1 |
115 | Faint yellow | 4.0 | 98.4 |
120 | Orange-yellow | 3.0 | 98.0 |
125 | Black | 2.5 | 95.3 |
135 | Black | 2.5 | 93.0 |