Reaction temperature (˚C)

Color

Reaction time (h)

Yield (%)

90

White

4.0

22.1

95

White

4.0

30.5

100

White

4.0

65.0

105

Faint yellow

4.0

98.0

110

Faint yellow

4.0

98.1

115

Faint yellow

4.0

98.4

120

Orange-yellow

3.0

98.0

125

Black

2.5

95.3

135

Black

2.5

93.0