Compound | Decomposition Step | Temperature Range (˚C) | Removes Species | Wt. Loss | |
% (Cacld.) | % Found | ||||
[V3O3(L1)(SO4)3(EtOH)1/2(H2O)3/2] (C19H18N6S3O17V3) | 1st | 27 - 263 | 1.5 H2O+1/2EtOH+N2 | 9.2 | 9.3 |
2rd | 263 - 329 | NO2+2H2 | 5.9 | 6.0 | |
3rd | 329 - 449 | 2SO4+C3H3+CO | 30.4 | 30.0 | |
4th | 449 - 598 | SO4+C9H5 | 24.6 | 24.7 | |
Residue | 598 - 800 | V3N3C5 | 30.0 | 30.0 | |
[VO(L1)(2,4-pentadionate)] Cl・4HCl (C23H23N6O3Cl5V) | 1st | 27 - 211 | 2HCl | 11.1 | 11.4 |
2nd | 211 - 398 | Cl+2HCl+2N2+O2+CO | 34.01 | 33.9 | |
3rd | 398 - 563 | C17H9N | 34.45 | 34.7 | |
Residue | 563 - 800 | C5H10NV | 20.5 | 20.0 | |
[V2O2(L1)(SO4)2(EtOH)5/2] (C23H27N6O25/2S2V2) | 1st | 28 - 207 | 1/2 EtOH+C | 4.7 | 4.8 |
2rd | 208 - 343 | 2EtOH+O2+N2+C2H4 | 23.9 | 23.9 | |
3rd | 343 - 422 | SO4+CH4 | 14.9 | 14.8 | |
4th | 422 - 565 | SO4+N2+2H2 | 17 | 17.3 | |
Residue | 565 - 800 | V2N2C14 | 39.6 | 39.2 | |
[VO(L1)SO4(H2O)3/2]・2.5H2O (C18H20N6SO9V) | 1st | 18 - 216 | 2.5 H2O | 8.23 | 8.5 |
2rd | 216 - 443 | 3/2 H2O+SO4+C5H5 | 34.4 | 34.5 | |
3rd | 443 - 574 | C9H5N5O | 36.4 | 35.9 | |
Residue | 574 - 1000 | C4H2NV | 21 | 20.8 | |
[V2O2(L1)(SO4)2(H2O)]・H2O (C18H16N6S2O12V2) | 1st + 2nd | 19 - 395 | 2 H2O+SO4 | 19.6 | 20.9 |
3rd | 395 - 448 | SO4+CH | 16.2 | 15.8 | |
4th | 448 - 525 | C14H5N4O2 | 38.7 | 38.2 | |
Residue | 525 - 1000 | C3H6N2V2 | 25.5 | 25.1 |