Br No.

Compound

Quantitation reference

Recoveries from spiked channel catfish (%)

Recoveries from spiked fish feeds (%)

2.5

10

25

10

40

100

Compounds using ¹³C ₁₂-BDE-77 as Labeled injection internal standard

3

BDE17

¹³ C ₁₂-BDE-28

92 ± 7

92 ± 5

96 ± 6

92 ± 5

103 ± 5

102 ± 6

3

BDE28

¹³ C ₁₂-BDE-28

87 ± 7

96 ± 5

94 ± 8

96 ± 5

101 ± 9

98 ± 9

4

BDE71

¹³ C ₁₂-BDE-47

74 ± 6

89 ± 10

95 ± 5

84 ± 6

101 ± 9

101 ± 7

4

BDE47

¹³ C ₁₂-BDE-47

87 ± 5

91 ± 7

96 ± 10

93 ± 7

99 ± 6

101 ± 7

4

BDE66

¹³ C ₁₂-BDE-47

78 ± 9

86 ± 5

93 ± 12

92 ± 10

101 ± 9

100 ± 9

5

BDE100

¹³ C ₁₂-BDE-100

82 ± 12

83 ± 6

95 ± 5

91 ± 8

103 ± 8

103 ± 8

5

BDE99

¹³ C ₁₂-BDE-99

81 ± 14

85 ± 7

94 ± 9

90 ± 11

96 ± 7

97 ± 5

5

BDE85

¹³ C ₁₂-BDE-99

78 ± 16

85 ± 6

87 ± 5

87 ± 5

95 ± 7

101 ± 6

Compounds using ¹³C ₁₂-BDE-138 as Labeled injection internal standard

6

BDE154

¹³ C ₁₂-BDE-154

74 ± 7

84 ± 6

89 ± 7

87 ± 8

96 ± 10

96 ± 11

6

BDE153

¹³ C ₁₂-BDE-153

75 ± 8

82 ± 4

90 ± 9

88 ± 9

90 ± 7

96 ± 10

6

BDE138

¹³ C ₁₂-BDE-153

75 ± 8

82 ± 4

85 ± 7

85 ± 7

87 ± 6

94 ± 7

7

BDE183

¹³ C ₁₂-BDE-183

83 ± 8

83 ± 3

85 ± 5

85 ± 4

97 ± 11

91 ± 7

7

BDE190

¹³ C ₁₂-BDE-183

—

80 ± 13

84 ± 5

—

91 ± 9

90 ± 5