Br No. | Compounds | Quantitation reference | Retention times (RT) (min) | Start time and end time of Retention Window (min) | No. of MS Scan Functions | LOQ | ||
Channel catfish (μg∙kg−1) | Fish feeds (μg∙kg−1) | |||||||
Compounds using | ||||||||
3 | BDE17 | | 14.11 | 13.44 - 14.53 | 2 | 0.25 | 1 | |
3 | BDE28 | | 14.92 | 14.24 - 15.40 | 4 | 0.25 | 1 | |
4 | BDE71 | | 19.69 | 18.93 - 20.05 | 5 | 0.5 | 2 | |
4 | BDE47 | | 20.37 | 19.66 - 20.87 | 6 | 0.5 | 2 | |
4 | BDE66 | | 21.36 | 20.64 - 21.88 | 8 | 0.5 | 2 | |
5 | BDE100 | | 25.06 | 24.27 - 25.55 | 11 | 1 | 4 | |
5 | BDE99 | | 26.68 | 25.96 - 27.05 | 13 | 1 | 4 | |
5 | BDE85 | | 29.35 | 28.61 - 29.88 | 14 | 1 | 4 | |
Compounds using | ||||||||
6 | BDE154 | | 30.76 | 29.86 - 31.06 | 16 | 1 | 4 | |
6 | BDE153 | | 33.02 | 32.23 - 33.37 | 18 | 1 | 4 | |
6 | BDE138 | | 35.81 | 35.02 - 36.20 | 20 | 2.5 | 10 | |
7 | BDE183 | | 39.00 | 38.22 - 39.33 | 22 | 2.5 | 10 | |
7 | BDE190 | | 42.19 | 41.46 - 42.57 | 23 | 5 | 20 | |
Labeled compounds | ||||||||
3 | | | 14.91 | 14.21 - 15.43 | 3 | — | — | |
4 | | | 20.38 | 19.68 - 20.87 | 7 | — | — | |
5 | | | 25.05 | 24.21 - 25.55 | 10 | — | — | |
5 | | | 26.67 | 25.93 - 27.14 | 12 | — | — | |
6 | | | 30.70 | 29.82 - 31.05 | 15 | — | — | |
6 | | | 33.00 | 32.20 - 33.35 | 17 | — | — | |
7 | | | 38.99 | 38.18 - 39.35 | 21 | — | — | |
Labeled injection internal standards | ||||||||
4 | | | 22.88 | 22.17 - 23.37 | 9 | — | — | |
6 | | | 35.80 | 35.00 - 36.25 | 19 | — | — | |