Br No.

Compounds

Quantitation reference

Retention times (RT) (min)

Start time and end time of Retention Window (min)

No. of MS Scan Functions

LOQ

Channel catfish (μg∙kg⁻¹)

Fish feeds (μg∙kg⁻¹)

Compounds using ¹³C ₁₂-BDE-77 as Labeled injection internal standard

3

BDE17

¹³ C ₁₂-BDE-28

14.11

13.44 - 14.53

2

0.25

1

3

BDE28

¹³ C ₁₂-BDE-28

14.92

14.24 - 15.40

4

0.25

1

4

BDE71

¹³ C ₁₂-BDE-47

19.69

18.93 - 20.05

5

0.5

2

4

BDE47

¹³ C ₁₂-BDE-47

20.37

19.66 - 20.87

6

0.5

2

4

BDE66

¹³ C ₁₂-BDE-47

21.36

20.64 - 21.88

8

0.5

2

5

BDE100

¹³ C ₁₂-BDE-100

25.06

24.27 - 25.55

11

1

4

5

BDE99

¹³ C ₁₂-BDE-99

26.68

25.96 - 27.05

13

1

4

5

BDE85

¹³ C ₁₂-BDE-99

29.35

28.61 - 29.88

14

1

4

Compounds using ¹³C ₁₂-BDE-138 as Labeled injection internal standard

6

BDE154

¹³ C ₁₂-BDE-154

30.76

29.86 - 31.06

16

1

4

6

BDE153

¹³ C ₁₂-BDE-153

33.02

32.23 - 33.37

18

1

4

6

BDE138

¹³ C ₁₂-BDE-153

35.81

35.02 - 36.20

20

2.5

10

7

BDE183

¹³ C ₁₂-BDE-183

39.00

38.22 - 39.33

22

2.5

10

7

BDE190

¹³ C ₁₂-BDE-183

42.19

41.46 - 42.57

23

5

20

Labeled compounds

3

¹³ C ₁₂-BDE-28

¹³ C ₁₂-BDE-77

14.91

14.21 - 15.43

3

—

—

4

¹³ C ₁₂-BDE-47

¹³ C ₁₂-BDE-77

20.38

19.68 - 20.87

7

—

—

5

¹³ C ₁₂-BDE-100

¹³ C ₁₂-BDE-77

25.05

24.21 - 25.55

10

—

—

5

¹³ C ₁₂-BDE-99

¹³ C ₁₂-BDE-77

26.67

25.93 - 27.14

12

—

—

6

¹³ C ₁₂-BDE-154

¹³ C ₁₂-BDE-138

30.70

29.82 - 31.05

15

—

—

6

¹³ C ₁₂-BDE-153

¹³ C ₁₂-BDE-138

33.00

32.20 - 33.35

17

—

—

7

¹³ C ₁₂-BDE-183

¹³ C ₁₂-BDE-138

38.99

38.18 - 39.35

21

—

—

Labeled injection internal standards

4

¹³ C ₁₂-BDE-77

¹³ C ₁₂-BDE-77

22.88

22.17 - 23.37

9

—

—

6

¹³ C ₁₂-BDE-138

¹³ C ₁₂-BDE-138

35.80

35.00 - 36.25

19

—

—