Bruker APEX diffractometer | 3009 Independent reflections |
Radiation source: graphite monochromated Cu-Kα radiation | 3009 reflections with I > 2 sigma(I) R(int) = 0.0497 |
Absorption correction: Semi-empirical from equivalents | θmax = 72.11˚, θmin = 3.20˚ |
Tmin =0.584652, Tmax =0.7939 | h= −12 → 10 |
4709 measured reflections | k = −9 → 8 |
| l = −17 → 17 |