Sample | Sb(III) Added (µg∙L−1) | Propose Methodology | ETTAS | RE%* | |
Sb(III) Found ± SD (µg∙L−1) | Recovery (%, n = 4) | Sb(III) Found ± SD (µg∙L−1) | |||
1 | - | 0.93 ± 0.03 | - | - | - |
0.36 | 1.278 ± 0.02 | 98.71 | |||
0.60 | 1.522 ± 0.07 | 99.14 | |||
2 | - | 0.77 ± 0.05 | - | 0.75 ± 0.09 | 2.60 |
0.36 | 1.134 ± 0.04 | 100.52 | |||
0.60 | 1.381 ± 0.03 | 101.43 | |||
3 | - | 1.88 ± 0.02 | - | 1.93 ± 0.03 | 2.59 |
0.36 | 2.231 ± 0.09 | 99.52 | |||
0.60 | 2.474 ± 0.07 | 99.68 | |||
4 | - | 1.32 ± 0.04 | - | 1.41 ± 0.04 | 6.38 |
0.36 | 1.685 ± 0.03 | 100.38 | |||
0.60 | 1.914 ± 0.03 | 99.55 | |||
5 | - | 0.65 ± 0.03 | - | 0.70 ± 0.001 | 7.14 |
0.36 | 1.008 ± 0.06 | 99.70 | |||
0.60 | 1.239 ± 0.08 | 98.31 | |||
6 | - | 1.13 ± 0.07 | - | 1.11 ± 0.03 | 1.77 |
0.36 | 1.476 ± 0.05 | 98.76 | |||
0.60 | 1.738 ± 0.04 | 100.70 | |||
7 | - | 1.06 ± 0.06 | - | 1.12 ± 0.02 | 5.36 |
0.36 | 1.431 ± 0.03 | 101.03 | |||
0.60 | 1.654 ± 0.02 | 99.43 | |||
8 | - | 1.45 ± 0.09 | - | - | - |
0.36 | 1.807 ± 0.01 | 99.79 | |||
0.60 | 2.055 ± 0.04 | 100.34 |