Component

Recovery results

(Mean % Recoverya ± % RSD)

LOQ level ; amount (% w/w)

50% of specification levelb;

amount (% w/w)

100% of specification levelb; amount (% w/w)

150% of specification levelb; amount (% w/w)

Imp-1

97.78

100.90

100.23

100.15

Imp-2

104.76

99.54

99.77

98.92

Imp-3

104.76

101.41

100.23

99.37

Imp-4

95.55

98.65

99.55

97.90

Imp-5

100.0

90.22

89.13

88.56

Imp-6

80.0

91.67

94.71

94.99

Imp-7

104.76

102.32

103.46

102.32

Imp-8

106.67

88.31

87.18

86.17