S. No.

Parameter

MON

DES

Peak area

Tailing factor

Peak area

Tailing factor

1

Initial Sample

2,812,194

1.164

3,423,037

1.060

2

Flow rate (+0.2 ml/min)

3,192,458

1.163

3,970,475

1.056

3

Flow rate (−0.2 ml/min)

2,412,494

1.164

3,174,376

1.047

4

Temp. change (10% more)

2,983,302

1.163

3,879,560

1.059

5

Temp. change (10% less)

2,355,063

1.167

3,052,650

1.055

% RSD

0.14

0.49