Sample | 2θ (˚) | d (Å) | | D (Å) | g (%) | α | FWHM | Delata E−03 |
PVA/PVP | 15.10 | 5.86 | 2.21 | 12.9 ± 0.6 | 1.5 | 9.9 ± 0.5 | 6.9 | 0.70 |
18.30 | 4.84 | 2.68 | 15.7 ± 0.8 | 0.5 | 1.8 ± 0.1 | 6.6 | ||
19.80 | 4.48 | 5.84 | 34.2 ± 1.5 | 0.0 | 1.1 ± 0.1 | 3.1 | ||
20.85 | 4.26 | 2.64 | 15.5 ± 0.7 | 0.5 | 1.7 ± 0.1 | 7.6 | ||
27.67 | 3.22 | 2.48 | 14.5 ± 0.6 | 0.5 | 2.0 ± 0.1 | 11.3 | ||
40.46 | 2.23 | 2.54 | 14.9 ± 0.7 | 0.5 | 2.5 ± 0.1 | 17.3 | ||
PVA/PVP + 0.2% CuSO4 | 15.04 | 5.88 | 2.22 | 13.0 ± 0.6 | 0.5 | 9.5 ± 0.5 | 6.9 | 1.08 |
19.93 | 4.45 | 4.24 | 24.8 ± 1.3 | 0.5 | 1.5 ± 0.1 | 4.4 | ||
21.77 | 4.08 | 2.56 | 15.0 ± 0.8 | 0.5 | 1.7 ± 0.1 | 8.3 | ||
26.56 | 3.36 | 2.47 | 14.5 ± 0.7 | 0.0 | 8.5 ± 0.4 | 10.8 | ||
40.33 | 2.23 | 3.26 | 19.1 ± 0.9 | 0.5 | 2.4 ± 0.2 | 13.1 | ||
16.16 | 5.48 | 2.19 | 12.8 ± 0.6 | 0.5 | 9.0 ± 0.4 | 7.5 | ||
PVA/PVP + 0.4% CuSO4 | 20.00 | 4.43 | 3.64 | 21.3 ± 1.0 | 1.0 | 1.4 ± 0.1 | 5.2 | 0.85 |
21.64 | 4.10 | 2.27 | 13.3 ± 0.7 | 0.0 | 9.9 ± 0.5 | 9.6 | ||
27.67 | 3.08 | 2.28 | 13.4 ± 0.7 | 0.5 | 8.2 ± 0.4 | 12.4 | ||
40.46 | 2.25 | 2.31 | 13.5 ± 0.7 | 0.0 | 9.2 ± 0.4 | 19.3 | ||
13.97 | 6.33 | 2.20 | 12.9 ± 0.6 | 0.0 | 9.1 ± 0.4 | 6.5 | ||
19.77 | 4.49 | 4.41 | 25.8 ± 1.3 | 0.5 | 1.6 ± 0.1 | 4.2 | ||
PVA/PVP + 0.6% CuSO4 | 21.62 | 4.10 | 4.01 | 23.5 ± 1.2 | 0.5 | 1.8 ± 0.1 | 5.1 | 1.56
|
29.84 | 2.99 | 2.14 | 12.5 ± 0.6 | 0.5 | 9.7 ± 0.5 | 15.2 | ||
40.42 | 2.23 | 2.61 | 15.3 ± 0.8 | 0.0 | 7.0 ± 0.4 | 16.8 | ||
16.52 | 5.36 | 2.25 | 13.2 ± 0.7 | 0.5 | 8.9 ± 0.5 | 7.4 | ||
19.74 | 4.49 | 3.23 | 18.9 ± 0.9 | 0.5 | 1.9 ± 0.1 | 5.9 | ||
22.03 | 4.03 | 2.43 | 14.2 ± 0.7 | 0.5 | 7.6 ± 0.4 | 8.9 | ||
PVA/PVP + 0.8% CuSO4 | 26.49 | 3.36 | 2.17 | 12.7 ± 0.6 | 0.5 | 9.0 ± 0.5 | 13.1 |
|
40.58 | 2.22 | 2.39 | 14.0 ± 0.7 | 0.5 | 2.2 ± 0.1 | 18.8 |
1.16 | |
16.58 | 5.34 | 2.20 | 12.9 ± 0.6 | 0.5 | 9.2 ± 0.5 | 7.7 | ||
19.74 | 4.49 | 3.43 | 20.1 ± 1.0 | 0.5 | 1.7 ± 0.1 | 5.5 | ||
22.23 | 3.99 | 2.86 | 16.8 ± 0.8 | 0.5 | 2.1 ± 0.1 | 7.6 | ||
29.05 | 3.07 | 2.57 | 15.1 ± 0.7 | 0.5 | 2.0 ± 0.1 | 11.5 | ||
PVA/PVP + 1.0% CuSO4 | 42.36 | 2.13 | 2.97 | 17.4 ± 0.8 | 0.5 | 3.0 ± 0.2 | 19.8 | 1.37 |
15.10 | 5.86 | 2.21 | 12.9 ± 0.6 | 1.5 | 9.9 ± 0.5 | 6.9 | ||
18.30 | 4.84 | 2.68 | 15.7 ± 0.8 | 0.5 | 1.8 ± 0.1 | 6.6 | ||
19.80 | 4.48 | 5.84 | 34.2 ± 1.5 | 0.0 | 1.1 ± 0.1 | 3.1 | ||
20.85 | 4.26 | 2.64 | 15.5 ± 0.7 | 0.5 | 1.7 ± 0.1 | 7.6 | ||
27.67 | 3.22 | 2.48 | 14.5 ± 0.6 | 0.5 | 2.0 ± 0.1 | 11.3 |