Sample

2θ (˚)

d (Å)

D (Å)

g (%)

α

FWHM

Delata E−03

PVA/PVP

15.10

5.86

2.21

12.9 ± 0.6

1.5

9.9 ± 0.5

6.9

0.70

18.30

4.84

2.68

15.7 ± 0.8

0.5

1.8 ± 0.1

6.6

19.80

4.48

5.84

34.2 ± 1.5

0.0

1.1 ± 0.1

3.1

20.85

4.26

2.64

15.5 ± 0.7

0.5

1.7 ± 0.1

7.6

27.67

3.22

2.48

14.5 ± 0.6

0.5

2.0 ± 0.1

11.3

40.46

2.23

2.54

14.9 ± 0.7

0.5

2.5 ± 0.1

17.3

PVA/PVP + 0.2% CuSO4

15.04

5.88

2.22

13.0 ± 0.6

0.5

9.5 ± 0.5

6.9

1.08

19.93

4.45

4.24

24.8 ± 1.3

0.5

1.5 ± 0.1

4.4

21.77

4.08

2.56

15.0 ± 0.8

0.5

1.7 ± 0.1

8.3

26.56

3.36

2.47

14.5 ± 0.7

0.0

8.5 ± 0.4

10.8

40.33

2.23

3.26

19.1 ± 0.9

0.5

2.4 ± 0.2

13.1

16.16

5.48

2.19

12.8 ± 0.6

0.5

9.0 ± 0.4

7.5

PVA/PVP + 0.4% CuSO4

20.00

4.43

3.64

21.3 ± 1.0

1.0

1.4 ± 0.1

5.2

0.85

21.64

4.10

2.27

13.3 ± 0.7

0.0

9.9 ± 0.5

9.6

27.67

3.08

2.28

13.4 ± 0.7

0.5

8.2 ± 0.4

12.4

40.46

2.25

2.31

13.5 ± 0.7

0.0

9.2 ± 0.4

19.3

13.97

6.33

2.20

12.9 ± 0.6

0.0

9.1 ± 0.4

6.5

19.77

4.49

4.41

25.8 ± 1.3

0.5

1.6 ± 0.1

4.2

PVA/PVP + 0.6% CuSO4

21.62

4.10

4.01

23.5 ± 1.2

0.5

1.8 ± 0.1

5.1

1.56

29.84

2.99

2.14

12.5 ± 0.6

0.5

9.7 ± 0.5

15.2

40.42

2.23

2.61

15.3 ± 0.8

0.0

7.0 ± 0.4

16.8

16.52

5.36

2.25

13.2 ± 0.7

0.5

8.9 ± 0.5

7.4

19.74

4.49

3.23

18.9 ± 0.9

0.5

1.9 ± 0.1

5.9

22.03

4.03

2.43

14.2 ± 0.7

0.5

7.6 ± 0.4

8.9

PVA/PVP + 0.8% CuSO4

26.49

3.36

2.17

12.7 ± 0.6

0.5

9.0 ± 0.5

13.1

40.58

2.22

2.39

14.0 ± 0.7

0.5

2.2 ± 0.1

18.8

1.16

16.58

5.34

2.20

12.9 ± 0.6

0.5

9.2 ± 0.5

7.7

19.74

4.49

3.43

20.1 ± 1.0

0.5

1.7 ± 0.1

5.5

22.23

3.99

2.86

16.8 ± 0.8

0.5

2.1 ± 0.1

7.6

29.05

3.07

2.57

15.1 ± 0.7

0.5

2.0 ± 0.1

11.5

PVA/PVP + 1.0% CuSO4

42.36

2.13

2.97

17.4 ± 0.8

0.5

3.0 ± 0.2

19.8

1.37

15.10

5.86

2.21

12.9 ± 0.6

1.5

9.9 ± 0.5

6.9

18.30

4.84

2.68

15.7 ± 0.8

0.5

1.8 ± 0.1

6.6

19.80

4.48

5.84

34.2 ± 1.5

0.0

1.1 ± 0.1

3.1

20.85

4.26

2.64

15.5 ± 0.7

0.5

1.7 ± 0.1

7.6

27.67

3.22

2.48

14.5 ± 0.6

0.5

2.0 ± 0.1

11.3