N˚ | 1 | 2 | ||
δC | δH | δC | δH | |
2 | 163.9 |
| 164.3 |
|
3 | 103.8 | 6.97 s | 103.1 | 6.85 s |
4 | 182.1 |
| 182.0 |
|
5 | 161.1 |
| 161.0 |
|
6 | 99.5 | 6.52 d (2.3) | 99.6 | 6.50 d (2.3) |
7 | 162.5 |
| 162.7 |
|
8 | 95.0 | 6.92 d (2.3) | 95.0 | 6.95 d (2.3) |
9 | 156.9 |
| 156.8 |
|
10 | 105.5 |
| 105.4 |
|
1' | 122.7 |
| 121.0 |
|
2', 6' | 128.4 | 8.07 d (8.7) | 128.6 | 7.98 d (8.7) |
3', 5' | 114.7 | 7.15 d (8.7) | 116.0 | 6.98 d (8.7) |
4' | 162.5 |
| 161.4 |
|
OCH3 | 55.6 | 3.88 s |
|
|
glucuronic acid |
|
|
|
|
1''' | 98.0 | 5.40 d (7.2) | 98.1 | 5.28 d (7.2) |
2'' | 82.2 | 3.58 m | 82.5 | 3.51 m |
3'' | 74.9 | 3.57 m | 75.4 | 3.52 m |
4'' | 70.8 | 3.49 t (9.4) | 71.3 | 3.32 t (9.4) |
5'' | 75.0 | 4.11 d (9.4) | 74.0 | 3.88 d (9.4) |
6'' | 170.0 |
| 171.0 |
|
glucose |
|
|
|
|
1''' | 104.6 | 4.49 d (7.8) | 104.8 | 4.48 d (7.8) |
2''' | 74.6 | 3.00 td (7.8, 3.4) | 74.7 | 3.00 td (7.8, 3.4) |
3''' | 76.2 | 3.20 td (8.8, 3.4) | 76.2 | 3.20 td (8.8, 3.4) |
4''' | 69.6 | 3.15 m | 69.6 | 3.12 m |
5''' | 76.9 | 3.16 m | 76.9 | 3.14 m |
6''' | 60.5 | 3.49 m | 60.5 | 3.45 m |