FE7 | 3630 (Ar-OH), 1669 (C=Ostr., ester), 3019 (C-H str., aromatic), 1569 (C=C skeletal str., phenyl), 1699 (C=C str., alkene), 1198 (C-O str. Ester), 2856 (C-H str., Ar-OCH3) 608.94 (long chain band) | 5.28 (1H s Ar-OH), 3.73-ArOCH3(s, 3H), 7.69 (d, 1H, C1of acrylate, j = 12 Hz), 6.49 (d, 1H, C2 of acrylate, , j = 12 Hz), 6.59 Ar-H (d, 1H j = 8 Hz) 6.84 Ar-H (d, 1H j = 20 Hz) 1.40 CH3 protons of t-butyl group (9H, s) | 149.9(C1), 150.3(C2), 117.3(C3), 155.7(C1’) 120.1(C2’) 167.5(C3’) 82.2(C4’) 28.9(C5’, C6’, C7’) | Molecular ion peak at 251 |
FE8 | 3625 (Ar-OH), 1689 (C=Ostr., ester), 3009 (C-H str., aromatic), 1565 (C=C skeletal str., phenyl), 1697 (C=C str., alkene), 1085 (C-O str. Ester), 2956 (C-H str., Ar-OCH3) 613.94 ( long chain band) | 5.280 (1H s Ar-OH), 3.943-ArOCH3(s, 3H), 7.086 (d, 1H, C1of acrylate, j = 3.6 Hz), 7.594 (d, 1H, C2 of acrylate, j = 1.6 Hz) 6.207 Ar-H(d, 1H j = 2 Hz) 6.944 Ar-H(d, 1H j = 2.4 Hz) 1.33 CH2 protons of pentyl chain(2H, m) 1.29 CH2 protons of pentyl chain (2H, m) 1.59 CH2 protons of pentyl chain (2H, m) 4.29 CH2 protons of pentyl chain (2H, m) 0.98 CH3protons of pentyl chain (3H, m). | 149.9(C1), 150.3(C2), 117.3(C3), 155.7(C1’) 120.1(C2’) 167.5(C3’) 65.4(C4’) 28.8(C5’). 28.1(C6’) 22.5(C7’) 14.1(C8’) | Molecular ion peak at 265 |
FE9 | 3625 (Ar-OH), 1689 (C=Ostr., ester), 3009 (C-H str., aromatic), 1565 (C=C skeletal str., phenyl), 1697 (C=C str., alkene), 1085 (C-O str. Ester), 2956 (C-H str., Ar-OCH3) 613.94 (long chain band) | 5.880 (1H s Ar-OH), 3.943-ArOCH3 (s, 3H), 6.086 (d, 1H, C1of acrylate, j = 25.6 Hz), 7.694 (s, 1H, C2 of acrylate) 6.207 Ar-H (d, 1H j = 2 Hz) 6.944 Ar-H (d, 1H j = 18 Hz) 1.40 CH2 of pentyl chain, (m 3H ) 4.13 (m, 1 H) CH of pentyl chain, 1.53 (m, 2H) CH2 of pentyl chain. 1.33 (m, 2H) CH2 of pentyl chain. 0.96 (t, 3H) CH3 of pentyl chain. | 149.9(C1), 150.3(C2), 117.3(C3), 155.7(C1’) 120.1(C2’) 167.5(C3’) 71.9(C4’) 21.8(C5’). 39.4(C6’) 16.4(C7’) 14.1(C8’) | Molecular ion peak at 265 |
FE10 | 3630 (Ar-OH), 1669 (C=Ostr., ester), 3019 (C-H str., aromatic), 1569 (C=C skeletal str., phenyl), 1687 (C=C str., alkene), 1152 (C-O str. Ester), 2966 (C-H str., Ar-OCH3) 570.94 (chlorine) | 5.880 (1H s Ar-OH), 3.943-ArOCH 3(s, 3H), 7.486 (d, 1H, C1of acrylate, j = 13.6 Hz), 7.524 (d, 1H, C2 of acrylate, j = 2 Hz) 6.507 Ar-H (d, 1H j = 4.4 Hz) 6.844 Ar-H (d, 1H j = 2.4 Hz) 4.41-CH2 (d, 2H, j = 3.6 Hz ) 3.66-CH2 (d, 2H, j = 24 Hz) | 149.9(C1) 155.3(C2) 127.3(C3) 151.9(C1’) 118.5(C2’) 173.5(C3’) 69.6(C4’) 42.4(C5’) | Molecular ion peak at 257 |
FE11 | 3615 (Ar-OH), 1699 (C=Ostr., ester), 3019 (C-H str., aromatic), 1569 (C=C skeletal str., phenyl), 1677 (C=C str., alkene), 1255 (C-O str. Ester), 2956 (C-H str., Ar-OCH3) 613.94 (bromine) | 5.680 (s, 1H, Ar-OH), 3.743-ArOCH3 (s, 3H), 6.41 (d, 1H, C1of acrylate, j = 16 Hz), 7.641 (d, 1H, C2 of acrylate, j = 20 Hz) 6.69 Ar-H (d, 1H, j = 3.2 Hz) 6.84 Ar-H (d, 1H, j = 20 Hz) 4.65 (d, 2H, CH2, j = 28 Hz ) 3.58 (d, 2H, CH2, j = 32 Hz) | 150.9(C1) 155.3(C2) 119.3(C3) 159.7(C1’) 119.1(C2’) 169.5(C3’) 70.6(C4’) 20.4(C5’) | Molecular ion peak at 302 |