Sample (wt%)

1st peak(˚C)

2nd peak(˚C)

3rd peak(˚C)

0

166.4

431.7

_

10

174.2

442.8

_

20

166.9

434.7

_

30

167.8

450.6

_

40

166.7

391.4

430.8

50

171.7

326.6

438.1