Source of Variation

Degree of freedom

Sum of

squares

Mean

Square

F-value

p-value

For 24 h

Regression Model

9

170.03

18.89

7.95

0.002

Residual

10

23.77

2.38

Total

19

193.80

Lack of fit

5

8.44

1.69

0.55

0.736

Pure Error

5

15.33

3.07

Summary of fit

R2 = 0.877

For 48 h

Regression Model

9

214.13

23.79

12.64

0.000

Residual

10

18.82

1.88

Total

19

232.95

Lack of fit

5

5.98

1.20

0.47

0.789

Pure Error

5

12.83

2.57

Summary of fit

R2 = 0.919

For 72 h

Regression Model

9

92.73

10.30

3.67

0.027

Residual

10

28.07

2.81

Total

19

120.80

Lack of fit

5

22.57

4.51

4.10

0.074

Pure Error

5

5.50

1.10

Summary of fit

R2 = 0.768