| Experimental Conditions |
| ||||
| Sample N | DA-HCl mass (mg) | VdiH2O (mL) | VNaOH /n:n(µl) | Rtemp (˚C) | dTEM (nm) |
| 1 | 180.00 | 90.00 | 760/1:0.65 | 40 | ~135 |
| 2 | 360.00 | 90.00 | 760/1: 0.32 | 50 | ~950 |
| 3 | 180.00 | 90.00 | 760/1:0.65 | 20 | ~170 |
| 4 | 153.18 | 79.59 | 400/1:0.40 | 40 | ~285 |
| 5 | 360.00 | 90.00 | 760/1:0.32 | 70 | ~1350 |
| 6 | 153.18 | 79.59 | 400/1:0.40 | 25 | ~180 |
| 7 | 119.70 | 90.00 | 312/1:0.40 | 30 | ~290 |
| 8 | 153.18 | 79.59 | 600/1:0.60 | 30 | ~275 |
| 9 | 180.00 | 90.00 | 094/1:0.80 | 50 | ~221 |
| 10 | 270.00 | 90.00 | 880/1:0.50 | 30 | ~650 |
| 11 | 360.00 | 90.00 | 1880/1:0.80 | 50 | ~520 |
| 12 | 180.00 | 90.00 | 760/1:0.65 | 30 | ~250 |