Crystal data

Chemical formula

C8H13Cl3N2Zn

Mr

308.92

Crystal system, space group

Monoclinic, P21/c

Temperature (K)

296

a, b, c (Å)

8.020 (3), 11.529 (4), 13.973 (4)

β (˚)

108.015 (2)

V (Å3)

1228.6 (7)

Z

4

Radiation type

Mo Kα

µ (mm−1)

2.62

Crystal size (mm)

0.17 × 0.11 × 0.09

Data collection

Diffractometer

Nonius Kappa CCD diffractometer

No. of measured, independent and observed [I > 2σ(I)] reflections

8636, 2912, 2308

Rint

0.038

(sin θ/λ)max−1)

0.657

Refinement

R[F2 > 2σ(F2)], wR(F2), S

0.032, 0.090, 1.06

No. of reflections

2912

No. of parameters

131

H-atom treatment

H-atom parameters constrained

Δρmax, Δρmin (e Å−3)

0.46, −0.50