| Sample | Size from TEM (nm) | Size from XRD (nm) | Lattice constants a and c (Å) |
| Z1 | DTEM = 27 ± 0.56 | D(100) = 22.3 D(002) = 30.8 D(101) = 22.5 | a = 3.2523 c = 5.2107 |
| Z2 | LTEM = 110 ± 1.03 DTEM = 35 ± 0.30 | D(100) = 29.8 D(002) = 50.7 D(101) = 30.8 | a = 3.2619 c = 5.2250 |
| Z3 | DTEM = 25 ± 0.3 | D(100) = 19.1 D(002) = 25.4 D(101) = 18.5 | a = 3.2602 c = 5.2221 |
| Z4 | LTEM = 97 ± 2 DTEM = 30 ± 0.50 | D(100) = 15.8 D(002) = 35.5 D(101) = 15.4 | a = 3.2594 c = 5.2211 |
| Z5 | DTEM = 19 ± 0.2 | D(100) = 17.7 D(002) = 23.6 D(101) = 17.3 | a = 3.2571 c = 5.2171 |
| Z6 | LTEM =87 ± 1 DTEM = 32 ± 2 | D(100) = 23.5 D(002) = 30.8 D(101) = 23.5 | a = 3.2591 c = 5.2211 |